Factory Direct Supply Lined Hydrothermal Synthesis Autoclave Reactor

Operation of the hydrothermal synthesis digestion tank.

1.Pour the reaction material into the PTFE bushing (temperature resistant to 200 degrees) or PPL para-polyphenyl bushing (temperature resistant to 280 degrees) and ensure that the filling factor is less than 0.8.
2.Make sure that the lower gasket of the kettle is correctly positioned (raised side down), then put in the PTFE bushing or PPL bushing and the upper gasket, tighten the kettle cover first, and then screw the kettle cover until it is twisted and tightened with a screw.
3.Place the hydrothermal kettle in the heater and raise the temperature to the required reaction temperature according to the specified heating rate. (less than the specified safe operating temperature).
4.Only open the lid of the kettle when it has been confirmed that the temperature inside the belly is below the boiling point of the solvent of the reactant species. When the reaction is finished and the temperature is cooled down, it is also necessary to strictly follow the prescribed cooling rate in order to ensure safety and the service life of the reactor.
5.After confirming that the temperature inside the belly is lower than the boiling point of the solvent of the reactant, first loosen the lid with the screw and then open the lid.
6.Clean the kettle in time after each use to avoid rust and corrosion. Take extra care to clean the sealing area of the kettle body and lid, and prevent them from being damaged by bruising.