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Fully Automated Distillation of Petroleum Products including Biofuels OptiDist - the Optimal Solution
The evaporating characteristics of hydrocarbons have an important effect on their performance. The D86 distillation method allows characterizing the tendency of a fuel to vaporize.
Eighty years combined experience of the companies Walter Herzog and ISL in designing and manufacturing automatic distillation equipment, directed PAC in the development of the most revolutionary automated distillation analyzer ever built.
OptiDist is the State-of-the-Art Optimal Solution for performing atmospheric distillation offering highest precision and ease of use ever seen. Only the OptiDist enables truly “one button” straightforward operation. To start a test you just select the boiling group of the sample and push the Start Button.
Superior Precision from the First Run
The OptiDist fully automatically sets the optimal distillation conditions for Initial Heating, Distillation and Final Heating for any sample through the unique heating optimizer technology. It delivers up to 2 times better precision for all common distillation samples. You get perfect results from the first run even for “unknown” samples!
Enhanced Instrument Features
The optimizer technology assures perfect repeatability of distillation conditions without any compromise. The optimized heating protects flask material from critical overheating, improves flask life-time and prevents from potential fire. The operator also benefits from the environmental-friendly design by the drastically reduced VOC emission.
Unparalleled Versatility
The versatile design enables multi-methods and non-standard capability and can easily be adapted for different applications. OptiDist can be run as Stand Alone Unit or it can be linked together with several units to a Server-PC. OptiDist offers flexible and customized test report with enhanced communication features to LIMS, any printer or a centralized database on a Server-PC with ALAN or HLIS software.
Methods
ASTM D86, D1078, D850
EN ISO 3405, ISO 918
IP 123, IP 195, DIN 51 751
JIS K2254, NF M07-002
Main Features
? Easy to use mistake proof unit
? Quick connection for flask
? Self positioning heater lift
? Automatic heater base plate detection
? One button straight forward operation
? Superior precision from the first run
? Measuring of the Charge Volume
? Enhanced instrument features
? Reduced VOC emission
? Stand Alone Unit or networked with a PC
? Compatible with HLIS or ALAN
? Customized Printer Reports
? Built in or external Printer
? Flexible LIM communication
? Small Foot Print
Specification
General Information
OptiDist is a compact self-contained instrument with factory filled CFC-free cooling system, delivered with all accessories to immediately begin testing. It includes 125ml flask, 100ml receiver, vapor probe with centering device, heater plates 38 and 50mm, flask connection silicone tube, receiver cap and condenser cleaner
Standard Test Methods
ASTM D86 (group 0,1,2,3,4), IP123, DIN 51751, NF M07-002, EN ISO 3405, JIS K2254, ASTM D850, D1078, IP195, ISO 918
10% Distillation Residue
OptiDist can create the 10% Distillation residue with 100 or 200ml sample which can be used for Carbon Residue Measurement according to the following methods: ASTM D189, D524, D4530, EN ISO 10370
Operation
User Interface
Flask Heating System
Distillation Rate
Condenser System
Receiving Chamber
Large graphic TFT-LCD color touch-screen with solvent-proof protection
Low mass and low voltage, self-positioning heating system
Unique Optimizer function for fully automatic initial heat settings, distillation rate regulation and final heating regulation; to start test select the group and push start button; automatic residue calculation
Distillation Rate regulation 2 to 10 ml/min
Temperature range from 0 to 65°C (32 to 149°F); programmable constant temperature, temperature ramping or special temperature profile; instantaneously ready at switch on; automatic cooling liquid level detection
Temperature range from 0 to 40°C (32 to 104°F); corrosion proof design; programmable temperature or automatic adjustment to sample charge temperature; compatible with 100ml and 200ml receiver cylinders
Measurements
Vapor Temperature
Sample Volume
Ambient Pressure
Range : 0 to 450°C (32 to 842°F); Accuracy: Pt 100 probe IEC 751 Class A Built in calibration memory with 10 point calibration table and automatic probe ID detection; optional calibration certificate
Optical measuring system compatible with samples producing smoke in the receiver cylinder; Range: 0 to 103% of charge volume; Resolution: 0,03ml; Accuracy: ± 0,1ml
Built-in pressure sensor; Range: 70 to 110kPa (500 to 800 mmHg)
Calibration: Single point against reference barometer; memory for calibration history
Safety
Fire Extinguisher
Reduction of VOC emission
Built in fire extinguisher with 2 fire sensors
Drastically reduced emission of VOC (Volatile Organic Compounds)
User Error Prevention
Detector for heater base plate type, detectors for vapor probe and centering device, detectors for “receiver cylinder in place” and “receiver chamber door open”, detector for “condenser cleaned”
Software functions
Operation as Stand Alone Unit or in a net ware with several units linked to a PC
Connection to external PC with HLIS or ALAN;
User defined Start procedure with quick start or start guide;
Result data base for 100 results;
QC data base for 5 samples and 250 results;
Product data base for 200 products with 33 specification points each;
Customized reporting on display, printer and LIMS
Measuring of the charge volume; automatic receiver temperature setting to the room temperature; automatic Diagnostic Function with 32 Alarms and message history
Calculations
Calculated Cetane Index, acc. D 4737 and D 976
Driveability Index acc. D 4814
Connectivity
3 * USB for external printer, barcode reader and memory stick
RS232C serial port for LIM connection
Ethernet RJ45 port for unit networking and connection to an external PC with ALAN or HLIS
Connectors for Ambient Temp. Sensor, Status indicator and for Unit Diagnostic
External Connections Fire extinguisher gas
VOC vent
Connection for Fire extinguishing gas CO2; Gas pressure 7±0,5 bar; Gas Flow rate 30 to 35 liters/s; Average volume used to extinguish a fire 150 liters; time to extinguish takes between 2 and 4 seconds
Fitting G1/4A for tube OD 8mm or for connection with hose nozzle and a hose with inside diameter of 8 mm
Built in Blower and connection for VOC vent
Operating Requirements
Temperature 10 to 35°C (50 to 95°F);
Relative humidity up to 80% at 35°C (95°F)
Multi Voltage 100 to 240V; 1400W
Dimensions and Weight
44cm W * 57cm D * 65cm H (17,3’’ * 22,4’’ * 25,6’’); 68kg (150lb)
Options & Accessories
Built-in Ticket Printer (only factory installation)
External printer
Barcode Reader
External status indicator
Ambient temperature sensor
Automatic dry point kit for 200cc
Automatic dry point kit for 125cc
Crude Oil testing capability (only factory installation)
Reduction of VOC emission (only factory installation)
200cc test kit for 10% Distillation Residue
Doctor Box
CRM reference materials
OptiDist basic unit and factory installed options
Ord.-No. Description
0101-004-001 OptiDist Automated Atmospheric Distillation Analyzer
100-240V AC, 50/60Hz, 1400W
Acc. to ASTM D 86, ISO 3405, IP 123, DIN 51 751, NF M07-002, JIS K2254 for boiling groups 0 - 4 Acc. to ASTM D 850, D 1078, IP 195.
With Optimizer for fully automated heater regulation
Stand alone unit with Colored Touch Screen and possibility to connect to a PC with HLIS or ALAN
With low voltage heater flask heater and fire extinguisher With factory filled sealed cooling system and with built-in CFC free cooler compressor.
Accessories included:
8013-004-00X Documentation CD
2002-004-001 OptiDist Measuring Cylinder 100ml with brass base
2201-004-001 OptiDist Flask 125ml
2001-004-008 OptiDist Vapor Probe Stopper for 100ml, 125ml and 250ml flask
3801-110-001 OptiDist Vapor Probe with calibration certificate calibrated at 50°C and 250°C
3002-004-1031 OptiDist Vapor Probe wire guide
3003-004-1007 OptiDist Vapor Probe holder
3002-004-1013 OptiDist Heater Base Plate 50 mm opening
3002-004-1014 OptiDist Heater Base Plate 38 mm opening
2007-004-009 OptiDist Silicone hose for flask connection
3004-004-1002 Rubber Cap for Measuring Cylinder
2000-004-002 OptiDist Condenser Cleaner
3001-004-1065 OptiDist Receiver Chamber Liquid Vessel
1700-000-007 Ethernet Cable 3m
3002-000-1002 Hose connection piece
5201-000-001 Set of hexagonal wrenches
0101-004-002 Same as 0101-004-001 but with built in Ticket Printer
0101-004-003 Same as 0101-004-001 but with built in Reduction of VOC emission and with Crude Oil testing capability
After the test VOCs (volatile organic compounds) are removed from the receiver chamber, through an outlet pipe on the back of the unit, with a built in blower Accessories included:
2201-004-005 OptiDist Flask 250ml
0101-004-004 Same as 0101-004-001 but with built in Ticket Printer, with Reduction of VOC emission and with Crude Oil testing capability
After the test VOCs are removed from the receiver chamber, through an outlet pipe on the back of the unit, with a built in blower
Accessories included:
2201-004-005 OptiDist Flask 250ml
OptiDist Measuring Cylinder Tube 200ml
O-Ring set Viton 30,8 * 3,6 for 200ml Measuring
Cylinder
Consists of:
2401-036-030801 Viton O-Ring 30,8 * 3,6
D86 RECEIVER, w/ GLASS BASE for ISL? OPTIDIST? instrument
D86 RECEIVER, w/ GLASS BASE for HERZOG? instrument
ASTM Petroleum Glassware
D86 Distillation of Petroleum at Atmospheric Pressure
D56 Flash Point by Tag Closed Cup Tester
D87 Melting Point of Petroleum Wax
D92 Flash and Fire Points by Cleveland Open Cup
D93 Flash Point by Pensky-Martens Closed Cup Tester
D97 Pour Point of Petroleum Products
D130 Copper Strip Test for Petroleum Products
D287 API Gravity of Petroleum Products Hydrometer Method
D381 Gum Content in Fuels by Jet Evaporation
D446 Glass Capillary Kinematic Viscometers
D473 Sediment in Crude and Fuel Oils by Extraction Method
D524 Ramsbottom Carbon Residue of Petroleum Products
D611 Aniline Point of Petroleum Products and Hydrocarbon Solvents
D525 Oxidation Stability of Gasoline
D665 Rust Preventing Characteristics of Inhibited Mineral Oil
D721 Oil Content of Petroleum Waxes
D892 Foaming Characteristics of Lubricating Oils
D942 Oxidation Stability of Lubrication Greases
D943 Oxidation Characteristics of Inhibited Mineral Oils
D1078 Distillation Range of Volatile Organic Liquids
D1160 Distillation of Petroleum Products at Reduced Pressure
D1217 Density of Liquids by Bingham Pycnometer
D1266 Sulfur in Petroleum Products
D1319 FIA System
D1401 Water Separability of Petroleum Oils and Synthetic Fluids
D2001 Depentanization of Gasoline and Napthas
D2007 Characteristic Groups in Rubber Extender and Processing Oils
D2386 Freezing Point of Aviation Fuels
D2500 Cloud Point of Petroleum Products
D2983 Low Temperature Viscosity by Brookfield Viscometer
D3242 Acidity in Aviation Turbine Fuel
D3427 Air Release Properties of Petroleum Oils
D4530 Determination of Carbon Residue (Micro Method)
D4636 Corrosiveness and Oxidation Stability
D6371 Cold Filter Plugging Point
D7279 Houillon Viscometer
PAC is the leading manufacturer of advanced analytical instruments for gas chromatography, elemental analysis, physical properties, and fuels composition. Our portfolio includes the world’s most respected brands of lab and process analyzers: AC Analytical Controls, Advanced Sensors, Alcor, Antek, Cambridge Viscosity, Herzog, ISL, PetroSpec and Phase Technology.
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