HK-RPP-2 Micro Coulometric Titrator
HK-RPP-2 Micro Coulometric Titrator
Overview
HK - RPP - 2 microcoulometric titrator can automatically compensate the baseline correction and do blank compensation. Conform to the standard of ASTM D6304 GB/T6283,GB/T11133, operating parameters and analysis results in addition to the digital tube display. And we can to print file according to user's actual requirement.
And our company latest develop one kind of titrant, with no pyridine or methyl alcohol in addition to have high sensitivity, good stability, accurate, simple operation, analysis the advantages of rapid, and can it can also eliminate the cartesian reeked of special reagent, usually to overcome the limitation of hygroscopic failure general reagent and prolong service life. Can be widely used in petroleum, petrochemical products in the analysis of the water content, can also be used in chemical, food, electric power, metallurgy, medicine, health and environmental protection system monitoring material moisture content.
Fundamental theory
HK - RPP - 2 microcoulometric titrator conforms to the micro coulometric titration principle, use double platinum electrode in detecting titration process, we use a microcomputer system to control electrolysis and data process with a new generation of intelligent microcoulometric titrator.
In the classical Karl fischer volumetric titration process, when water exists, iodine and sulfur dioxide will occur the following reaction.
H2O+I2+SO2+CH3OH+3RN→2RN· HI+RN· HSO4CH3…………………………………(1)
user adds the iodine standard solution as reaction needed iodine.
Our HK - RPP – 2 is a new generation of coulometric titrator, which is based on the sample containing iodine special solvent soluble electrolyte, water consumption of iodine, iodine is no longer required for using standard iodine titration reagent, but by electrolytic process to make the solution of iodine ion in anode oxidation for iodine
2I—2e→I2…………………………………………………………………………(2)
The reacted iodine and the water in the sample got reaction, it indicates the final point with double platinum electrode. When the iodine concentration in the titrant recovers to original, it stops electrolysis. Then according to Faraday's l electrolysis law.
In the formula :m——, water weight in the samplemg
C ——Electrolytic consumption of electricity,mc;
M——water molecular weight;
n——electron transfer number;
i——electrolytic current,mA;
t——Electrolytic time,S;
96500——Faraday's constant
10722——electricity consumption to electrolyze 1mg water,mc.
Only input all required parameters into the microcomputer, the titrator can give final result automatically. The testing unit can be shown by ppm, %, μg or mc.
Technical Parameters
1, measuring method:microcoulometric titration
2, measuring range:sample water content is from 1μg to 80mg
3, precision: 0.1μg
4, Accuracy degree:±5%±1μg
5, electrolytic manner:pulse current,Positive and negative electrolysis function
6, compensation way:automatic Postive and negative background compensation
7, control system:MCS—51 SCM control system
8, final point display:Electronic alarm instructions
9, result display: big LCD screen can display ppm,%,μg and mc.
10, printing method:16 characters, can print results continuously.
11, final point detection:double-platinum electrode indication
12, titration cell volume:150mL
13, stirring way:magnetic stirrers
14, power supply:220V±10%,50Hz
15, power:50W
16, ambient temperature:10℃~40℃
17, humidity:≤75%
Standard Configuration
No. |
Name |
Specifications |
Unit |
Qty |
1 |
Main host |
|
Set |
1 |
2 |
electrolytic tank |
|
Piece |
1 |
3 |
anolyte |
|
Bottle |
1 |
4 |
injection syringe |
50ml |
Piece |
1 |
5 |
injection syringe |
5ml |
Piece |
1 |
6 |
injection syringe |
0.25ml |
Piece |
1 |
7 |
injection syringe |
100μl |
Piece |
1 |
8 |
injection syringe |
10μl |
Piece |
1 |
9 |
injection syringe |
1μl |
Piece |
1 |
10 |
rubber pad |
|
Piece |
10 |
11 |
Power wire |
|
Piece |
1 |
12 |
Fuse |
2A |
Piece |
2 |
13 |
Print paper |
|
Roll |
2 |
14 |
Certificate |
|
Piece |
1 |
15 |
Manual |
|
Piece |
1 |
16 |
warranty card |
|
Piece |
1 |
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